DB4401/T 102.4-2020 建设用地土壤污染防治 第4部分：土壤挥发性有机物监测质量保证与质量控制技术规范

ICS13.080

CCSZ10DB4401

广州市地方标准

DB4401/T102.4—2020

建设用地土壤污染防治

第4部分：土壤挥发性有机物监测质量保

证与质量控制技术规范

Soilpollutionpreventionandcontroloflandforconstruction—

Part4:Technicalspecificationsforqualityassuranceandquality

controlforsoilvolatileorganiccompoundsmonitoring

2020-10-10发布2020-11-15实施

广州市市场监督管理局联合发布

广州市生态环境局

DB4401/T102.4—2020

目  次

前言.....................................................................................................................................................................III

引言.......................................................................................................................................................................Ⅴ

1范围...................................................................................................................................................................1

2规范性引用文件...............................................................................................................................................1

3术语和定义.......................................................................................................................................................1

4人员...................................................................................................................................................................2

4.1现场监测人员............................................................................................................................................3

4.2实验室分析、校核人员............................................................................................................................3

4.3报告审核人员............................................................................................................................................3

4.4报告签发人员..............................................................................................................................................3

5仪器与设备.......................................................................................................................................................3

5.1采样设备....................................................................................................................................................3

5.2现场快速检测设备....................................................................................................................................3

5.3实验室检测设备........................................................................................................................................4

6样品采集...........................................................................................................................................................4

6.1点位布设....................................................................................................................................................4

6.2采样孔位置与深度....................................................................................................................................4

6.3采样............................................................................................................................................................4

6.4样品保存和流转........................................................................................................................................5

6.5现场记录....................................................................................................................................................5

6.6现场质量控制样品....................................................................................................................................5

7实验室分析.......................................................................................................................................................6

7.1设施和环境条件........................................................................................................................................6

7.2分析方法....................................................................................................................................................6

7.3样品制备....................................................................................................................................................6

7.4试剂和材料................................................................................................................................................6

7.5样品分析....................................................................................................................................................6

7.6实验室质量控制........................................................................................................................................7

7.7记录与报告................................................................................................................................................8

8质量监督计划...................................................................................................................................................8

9质控数据统计...................................................................................................................................................9

附录A（资料性）主要检测分析方法测试精密度和准确度允许范围.......................................................10

附录B（资料性）质控数据统计表...............................................................................................................11

I

DB4401/T102.4—2020

前  言

本文件按照GB/T1.1—2020《标准化工作导则第1部分：标准化文件的结构和起草规则》的规定起

草。

本文件为DB4401/T102的第4部分。DB4401/T102拟分为以下部分：

——第1部分：污染状况调查技术规范

——第2部分：污染修复方案编制技术规范

——第3部分：土壤重金属监测质量保证与质量控制技术规范

——第4部分：土壤挥发性有机物监测质量保证与质量控制技术规范

……

本文件由广州市生态环境局提出并归口。

本文件起草单位：广州市环境监测中心站、广州检验检测认证集团有限公司、广州市环境技术中心。

本文件主要起草人：胡丹心、张蕖、何文祥、周展锋、李芳芳、周志洪、陈敏毅、魏