DB4401/T 102.5-2021 建设用地土壤污染防治 第5部分：土壤半挥发性有机物监测质量保证与质量控制技术规范

ICS13.080

CCSZ10DB4401

广州市地方标准

DB4401/T102.5—2021

建设用地土壤污染防治

第5部分：土壤半挥发性有机物监测质量

保证与质量控制技术规范

Soilpollutionpreventionandcontroloflandforconstruction—

Part5:Technicalspecificationsforqualityassuranceandquality

controlforsoilsemivolatileorganiccompoundsmonitoring

2021-12-30发布2022-02-01实施

广州市市场监督管理局联合发布

广州市生态环境局

DB4401/T102.5—2021

目次

前言.......................................................................................................................................................................Ⅱ

引言.......................................................................................................................................................................Ш

1范围...................................................................................................................................................................1

2规范性引用文件...............................................................................................................................................1

3术语和定义.......................................................................................................................................................1

4人员...................................................................................................................................................................2

4.1现场监测人员............................................................................................................................................2

4.2实验室分析、校核人员............................................................................................................................2

4.3报告审核人员............................................................................................................................................2

4.4报告签发人员............................................................................................................................................2

5仪器与设备.......................................................................................................................................................2

5.1采样设备....................................................................................................................................................2

5.2实验室检测设备........................................................................................................................................2

6样品采集...........................................................................................................................................................3

6.1点位布设....................................................................................................................................................3

6.2采样孔位置与深度....................................................................................................................................3

6.3采样............................................................................................................................................................3

6.4样品保存和流转........................................................................................................................................3

6.5现场记录....................................................................................................................................................3

6.6现场质量控制样品....................................................................................................................................4

7实验室分析.......................................................................................................................................................4

7.1设施和环境条件........................................................................................................................................4

7.2分析方法....................................................................................................................................................4

7.3试剂和材料................................................................................................................................................4

7.4试样的制备................................................................................................................................................5

7.5样品分析....................................................................................................................................................5

7.6实验室质量控制........................................................................................................................................6

7.7记录与报告................................................................................................................................................7

8质量监督...........................................................................................................................................................8

9质控数据统计...................................................................................................................................................8

附录A（资料性）主要分析方法测试的质控要求...........................................................................................9

附录B（资料性）质控数据统计表..................................................................................................................10

Ⅰ

DB4401/T102.5—2021

前  言

本文件按照GB/T1.1—2020《标准化工作导则第1部分：标准化文件的结构和起草规则》的规定起

草。

本文件为DB4401/T102的第5部分。DB4401/T102已发布以下部分：

——第1部分：污染状况调查技术规范；

——第2部分：污染修复方案编制技术规范；

——第3部分：土壤重金属监测质量保证与质量控制技术规范；

——第4部分：土壤挥发性有机物监测